B.Tech. Prospectus No. 031760

V to VIII Semester

AMRAVATI UNIVERSITY

(Faculty of Engineering & Technology)

PROSPECTUS

Prescribed for

four year Degree Course

Bachelor of Technology

(Chemical Engineering)

V to VIII semester

Examinations, 2002-03 & 2003-04

(semester Pattern)

2002

Price Rs. 16/-

PUBLISHED BY

Dr.P.S.Narkhede

Registrar

Amravati University,

Amravati 444 602

AMRAVATI UNIVERSITY

SPECIAL NOTE FOR INFORMATION OF THE STUDENTS

(1) Notwithstanding anything to the contrary, it is notified for general information and guidance of all concerned that a person, who has passed the qualifying examination and is eligible for admission only to the corresponding next higher examination as an ex-student or an external candidate, shall be examined in accordance with the syllabus of such next higher examination in force at the time of such examination in such subjects, papers or combination of papers in which students from University Departments or Colleges are to be examined by the University.

(2) Be it known to all the students desirous to take examination/s for which this prospectus has been prescribed should, if found necessary for any other information regarding examinations etc., refer the University Ordinances Booklet the various conditions/ provisions pertaining to examinations as prescribed in the following Ordinances -

Ordinances No.1 : Enrollment of Students.

Ordinances No.2 : Admission of Students

Ordinances No.4 : National Cadet Corps

Ordinances No.6 : Examination in General (relevant extracts)

Ordinance No.7-A ; Condonation of Deficiency of Marks for passing an Examination or for improvement of Division there at in the Faculties of Arts, Science, Commerce, Education, Social Science, Law, Home Science and Engg. & Technology and Examinations in Pharmaceutical Sciences.

Ordinance No. 7-B ; Condonation of Deficiency of Marks for Passing an Examination in the faculty of Medicine (Excluding examinations in Pharmaceutical Science)

Ordinance No. 9 : Conduct of Examinations (Relevant Extracts)

Ordinance no.10 : Providing for Exemptions and Compartments.

Ordinance No.19 : Admission of Candidates to Degrees

Ordinance No.109 : Recording of a change of name of a University Student in the records of the University.

Ordinance No.138 : For improvement of Division.

Ordinance No.159 : Prescribed rules for Revaluation of Answer Books of Examinees at University Examinations.

Dr.P.S.Narkhede

Registrar

Amravati University.

PATTERN OF QUESTION PAPER ON THE UNIT SYSTEM

The Pattern of question paper as per unit system will be broadly based on the following pattern

(1) Syllabus has been divided into units equal to the number of question to be answered in the paper. On each Unit there will be a question either a long answer type or a short answer type.

(2) Number of question will be in accordance with the unit prescribed in the syllabi for each paper i.e. there will be one question on each unit.

(3) For every question long answer type or short answer type there will be an alternative choice from the same unit. However, there will be no internal choice in a question.

(4) Division of marks between long answer and short answer type question will be in the ratio of 40 and 60.

(5) Each short answer type question shall contain 4 to 8 short sub question with no internal choice.

syllabus

prescribed for

B.Tech. (Chemical Engg.)

Fifth semester

5 SCECT 1 HEAT TRANSFER

SECTION-A

Unit I : Importance of heat transfer in chemical process industries. Modes of heat transfer, steady state conduction in one dimension.

Fourier’s law.

Heat transfer through plane, cyclindrical and spherical walls, compound resistance in series, thermal insulation, critical and economic thickness. Extended surface equipments, types, their design & operation, introduction to unsteady state heat transfer.

Unit II : Heat transfer by convection, film concept, individual and overall coefficients and factors affecting them. Natural and forced convection dimensional analysis applied to heat transfer. Dittus-Boelter equation. Limitations and application.

Unit III : Heat transfer by parallel and counter current flow, concept of log mean tempeature difference, rate of heat transfer. Heat transfer by film wise and dropwise condensation in horizontal & vertical tube.

SECTION-B

Unit IV : Heat exchange equipments and their design, double pipe, parallel, counter current, shell and tube heat exchangers, condensers, fouling factors, concepts of transfer units in heat exchangers, NTU concept for heat exchangers.

Unit V : Boiling & Evaporators : Classification of types and field applications of evaporators single and multiple effect evaporators.

Heat transfer through submerged coils, jacketted vessels.

Unit VI : Heat transfer by radiation, concept of black body, Kirchoff’s law, Stefan’s law, Black and gray body radiation, view factors luminous and non-luminous gases. Heat transfer in packed and fluidised beds.

Recent developments in heat transfer.

PRACTICALS : Based on above syllabus.

BOOKS RECOMMENDED :

1) Heat Trasnfer : Mc Adams

2) Heat Transfer : Sukhatme

3) Basic Heat Transfer : Necati Orisik, McGraw Hill Co., Kogakusha.

4) Heat Transfer : J.P.Hokman, McGraw Hill Co., Kogakusha.

5) Unit Operations of : McCab and Smith.

Chemical Engg.

6) Introduction to : Bedger and Banchero.

Chemical Engg.

7) Chemical Engg. : Coulson & Richardson, Vol. I (ELBS, Pergamon Press, 1970)

8) Heat Transfer : Gebhart, McGraw Hill,

2nd edition, 1979.

9) Fundamentals of Engg. : R.C.Sachdeva, Wiley Eastern.

10) Heat Transfer : R.C.Sachdeva.

5 SCE (FPOPC) T3 CHEMICAL ENGINEERING THERMODYNAMICS

SECTION-A

Unit I : Scope of thermodynamics and its importances to chemical Engineers, Basic concepts, extensive & intensive properties. state function & chemical systems. Definition, symbols & interrelation, concepts of Entropy, Enthalpy & internal energy. First law of thermodynamics, Equations of state, critical properties, Vander Wall’s constants, Virial expansions, Redlich-Kwong equation, Beattie-Bridgeman equation.

Unit II : First law applied to thermodynamic processes & calculation of Workdone, free energy & heat changes. Maxwell relation equation, second law and third law of thermodynamics. Thermodynamics relations based on second law. Relation between Cp & Cv, compressibility factor & coefficient of thermal expansion, concept of residual entropy & entropy of equilibrium.

Unit III : Partial molar and apparent molar properties, Gibbs Duhem equation, Chemical potential, effect of temperature and pressure fugacity, excess thermodynamic properties and thermodynamic properties of mixing. Gibbs-Duhem-Morgules equation, Konovalov laws. Colligative properties. Ebulliometric constant. Determination of Molecular Weight of unknown chemical substances. Solubility law.

SECTION-B

Unit IV : Vapour liquid equilibrium, T-X-Y diagrams & X-Y diagram for ideal & non ideal system. Raoult’s law and Henry’s law. Deviations from Raoult’s law. Comparision of ideal & non-ideal systems. Phase equilibria in non reaching multi-comonents, Binary, ternary systems. Graphical representation of L/L, L/S & G/S systems. Right angled triangular diagrams. Equilateral triangular diagrams, Janecke diagram, Effect of temp. & pressure on ternary equilibrium, Phenol-Wafer systems. auiline-water-chlorobenzene systems.

Unit V : Statistical thermodynamics, thermodynamics probability, its relation with Entropy, partition function and its relation with termodynamics functions, the Boltzman distribution law, Distribution law for chemically reactive system. Thermodynamics charts & their uses. Searching of thermodynamics data.

Unit V : Chemical Equilibrium, feasibility of chemical reaction, free energy change, Reaction co-ordinate, equilibrium constant, Effect of temp. & pressure, Relation between Kp, Kc & Kv, Le-Chatelier’s principle, Endo-Exothermic relations, Heterrogeneous equilibria, various methods of calculating free energy charge. Equilibrium conversiions, case study of feasibility report for manufacture of industrial chemicals.

BOOKS :

1) An Introduction to Chemical : R.P.Rastogi, R.R.Misra.

Thermodynamics

2) Chemical Engineering Process : Houghen-Watson.

3) Introduction to Chemical Engg. : J.M.Smith, H.C.Vauhess

Thermodynamics

4) Thermodynamics for : H.C.Weber, J.P.Meissner

Chemical Engg.

5) Engineering Thermodynamics : P.K.Nag.

*****

5 SCE 4 INORGANIC CHEMICAL TECHNOLOGY

(CHEMICAL ENGINEERING PROCESS-I)

SECTION-A

Unit I : Mineral based chemical process : Lime Magnesia, Cement, Phosphorous, Ceramic and Glass industries. Refractories.

Unit II : Industrial Processes for the production of acids, alkalies, salts, sulphuric acid, nitric acid, hydrochloric acid, soda ash, ammonia, etc.

Unit III : Fertilizers - Nitrogenous, Phosphatic and Potassium fertilizer. Sugar, Starch and Cellulose and Paper.

SECTION-B

Unit IV : Glyceride oils, Soaps, Glycerine, Surfactants resins and essential oils and alkaloids.

Unit V : Principle of electro-chemical technological process. Electrolytic process in agneous and molten system caustic soda chlorine.

Unit VI : Electrothermal industries, Aluminium, Magnesium, Litfium Titanium etc., Electro-chemical sources of energy and storage.

Note : Subject be taught with reference to Stoichiometry Thermodynamics, Kinetics, Chemical Engineering principles involved.

BOOKS RECOMMENDED :

1) Chemical Process Industries : R.N.Shreve, McGraw Hill, 1967.

2) Electro-Chemical Engineering : C.I.Mante, McGraw Hill, 1960.

3) Chemical Technology Manual, Chemical Tech., Vol. III,

Ed. D.Venkateshwarhe, Chemical Engg. Ed. Dev. Centre, 117, Madras.

4) Outline of Chemical Technology : C.E.Deyden,

Affiliated East-West Press, 1973.

*****

5 SCECT 5 ECONOMICS AND MANAGEMENT

SECTION-A

Unit I : Nature and Scope of Economics, introduction to managerial economics.

Demand concepts : Demand specification, types of demand.

Demand analysis : Significance of demand analysis, law of diminishing utility, Consumer’s surplus.

Demand forecasting : Concept of forecasting, types of forecasts, steps in demand forecasting, techniques of demand forecasting. (8)

Unit II : Meaning of Management, Principles of management, meaning and principles of scientific management, levels of management, delegation and authority,

Organisation, forms of organisation. (8)

Unit III : Production Concept, production function, Laws of return, scales of production, factors of production, production planning and control : Its meaning, essential factors for the success of production planning and control. (8)

SECTION-B

Unit IV : Capital Structure : Factors influencing the capital structure.

Types of capital, formation of capital, fixed capital, working capital.

Sources of Finance

Banking and Credit structure in India : Financial institutions, promotional polices and programmes of industrialisation, functions of Commercial Banks, functions of Central Bank. (8)

Unit V : Economic and Social Environment : Brief idea about economic environment of business, socio-cultural environment, Health hazards of chemical industries, awareness about AIDS & other diseases.

Brief idea about controls and regulation in India, Industrial licensing policy.

Glogalisation, Libertion and their effects.

Foreign exchange flow regulations, foreign technologies and company in India. (8)

Unit VI : Entrepreneur and Entrepreneurship :

Entrepreneurial competencies, institutional interface for small scale enterprises, opportunity scanning and identification.

Market assessment for SSE, choice of technology and selection of site, Ownership structure and organisational framework, preparation of business plan, main features of Indian factories act & minimum wage act.

Taxation in India. (8)

BOOKS RECOMMENDED :

1) Managerial Economics : K.K.Seo, Richard D. Irwin Inc.

2) Engineering Economics : J.L.Riggs, McGraw Hill, New York,

2nd edition, 1982.

3) Managerial Economics : Adhikary M., Khosla Pub. House, New Delhi.

4) Small Business Management Fundamentals : Dan Strenhoff and

J.F.Burgess, McGraw Hill Book Company.

5) Effective Small Business Management : Richard M.Hodgills,

Academic Press Incorporated, Harcourt, Brace Jovanovich.

6) Marketing Management for Small Units : Jain Vijay K.,

Management Publishing Co., 1988.

7) Marketing Management :- Analysis, Planning, Implementation and

Control : Kotler, Phillip, Prentice Hall of India Pvt. Ltd., 6th ed.,

1988.

8) Modern Economics Theory : K.K.Dewett.

*****

6 SCE 1 CHEMICAL ENGINEERING OPERATION

(MASS TRANSFER-I)

SECTION-A

Unit I : Importance of Mass Transfer Operation.

Classification of mass transfer, operations based on gas-liquid-solid contacts. Concepts of flux, resistance, driving force, equilibrium, direction of mass transfer, Dimensionless nos. in mass transfer.

Diffusion, Fick’s law I and II, Dependence of diffusivity on physical properties, Schmidt’s no. calculation, Determination of diffusivity in liquid-liquid, gas-gas, gas-liquid diffusion.

Unit II : Interphase mass transfer, various coefficient of mass transfer and their determination, resistance concept, controlling phase concept, Mass transfer in turbulent flow, Analogies of mass transfer, Empirical equations.

Theories of mass transfer, two film theory, Higbies penetration theory, Derivation of flux equation, surface renewal theory, Applications and problems.

Unit III : Absorptions, stagewise absorption, material balance overall, stepwise minimum irrigation rate, Absorption and stripping factor calculation of no. of stages, McCabe-Thiele graphical method, Kremsor-Brown-Sounder’s equation.

Equipments of absorption, tray towers, packed towers.

Continuous absorption, concept of H.T.U., N.T.U., H.E.T.P., comparision with stepwise columns, design concepts, determination of ht. and diameter of packed absorption column.

SECTION-B

Unit IV : Adsorption : Adsorption equilibria, types of adsorption, properties of adsorbents, single and multi-stage adsorption, adsorption isotherms, principles of adsorption, Break through curves, Adsorption of liquids, Basic equations, Adsorber design. Adsorption equipments.

Ion Exchange : Principles of ion exchange, Techniques and applications, Ion exchange equilibria, Rate of ion exchange.

Unit V : Drying and humidification.

Principles of drying, phase equilibrium, cross circulation drying, through circulation drying, drying of suspended particles, rate of drying curve, dryers for solids and pastes, dryers for solutions and slurries i.e. various types of dryers

Humidification : Terms, definitions, wet bulb temp., dry bulb temp. and measurement of humidity, Adiabatic saturation temp., study of temp humidity chart, Enthalpy-humidity charts, Determination of humidity, and concept of dehumidification. Equipments for humidification operations.

Unit VI : Crystallisation : Principles of crystallisation, Equilibria, calculation of yield, heat effects, crystal growth, properties of crystals nucleation, fractional crystallisation, caking of crystals, Various types of crystallise’s and their applications.

Membrane separation process, Types of membrane, separation of gases, separation of liquids, Dialysis, Reverse Osmosis pervaporisation, Desalination.

Recent Developments in Mass Transfer Operation.

PRACTICALS : Based on above syllabus.

BOOKS RECOMMENDED :

1) Unit Operation in Chemical Engg. : W.L.McCabe & J.C.Smith, McGraw Hill.

2) Mass Transfer Operation : R.E.Treybal.

3) Mass Transfer : T.K.Sherwood, R.I.Pigford, McGraw Hill.

4) Chemical Engg. : Coulson & Richardson.

*****

6 SCE (FPOPC) T 2 PROCESS EQUIPMENT DESIGN & DRAWING

SECTION-A

Unit I : Material behaviour under stresses, theories of failures. (8)

Unit II : Fabrication methods and their effects : Design method for atmospheric storage vessels, unfired pressure vessel subjected to internal and external pressure. (8)

Unit III : Vessels for high pressure operations, Agitated vessels. Tail columns, internals of the reactors. (8)

SECTION-B

Unit IV : Design of prcess equipment accessories and support systems. (8)

Unit V : Complete design and preparation of working drawing for typical process equipment, such as large storage vessels, thick wall pressure vessels. Self supported tall columns, agitated pressure vessels with heat transfer requirements etc. (8)

Unit VI : Design and layout of piping system and preparation of piping diagram for a typical process. Material selection and piping coding. (8)

PRACTICALS : Based on the above syllabus.

BOOKS RECOMMENDED :

1) Process Equipment Design : I.E.Brownell, E.H.Young, John Wiley, 1968.

2) Process Equipment Design : M.V.Joshi, McMillan, 1976.

3) Introduction to Chemical Engg. Design, Mechanical Aspects :

4) I.S.Code for Unfired Pressure : IS No. 2825 - 1969 pressure vessel.

5) Process Equipement Design & Drawing : S.D.Dawale.

6) International & Indian Standard codes for Piping.

*****

6 SCECT 3 INSTRUMENTATION & CONTROL

SECTION-A

Unit I : Measuring Instruments : Theories, practice and applications of measurements of temperature, mass and levels. (8)

Unit II : Measurement of pressure, vacuum, humidity & pH in process industry. (8)

Unit III : Methods for composition analysis. Principle and techniques of instruments for composition analysis in process industry, such as chromatography, spectroscopy, refractrometry etc. (8)

SECTION-B

Unit IV : Flow measuring instruments : Flow measuring devices for incompressible and compressible fluids. Electro-hydraulic valves, hydraulic servomotors, electro-pneumatic valves. Pneumatic actuators. (8)

Unit V : Introduction to Simple system analysis : Laplace Transformation. Block diagrams, linearization. First and higher order system. (8)

Unit VI : Frequency response, distributed parameter system, dead time.

Feed back control, servo and regulator control. Time domain closed loop responses, closed loop frequency response.

BOOKS RECOMMENDED :

1) Industrial Instrumentation : Eckman, Wiley Eastern

2) Instrumental Methods of Chemical Analysis : Erwing, McGraw Hill.

3) Instrumentation & Process Measurements : W.Bottom, Orient Longman.

4) Industrial Control & Instrumentation : W.Bottom, Orient Longman.

5) Outlines of Chemical Instrumentation & Process Control :

A. Suryanarayan, Khanna Pub., New Delhi.

*****

6 scect 5 COMPUTER APPLICATION IN CHEMICAL ENGINEERING

Note : Application of the following techniques for problems of interest in chemical engineering, writing and testing of programs written in C Language.

SECTION-A

Unit I : Numerical solution of first order differential equations with initial condition, Euler’s method, Runge-Kutta method.

Unit II : Systems of linear equations, solution by the method of determinants, matrix inversion for the solution of linear equations, Gauss elimination method.

Unit III : Roots of algebric and transcendental equation, iteration methods, Regula-Falsi method, Newton-Raphson method, roots of simultaneous and solution set of transcendental and algebric equations. Development of equations for heat transfer, fluid mechanics and reaction engineering problems.

SECTION-B

Unit IV : Regression analysis - Least Square, error approach, approximation by Chebychev orthogonal polynomial.

Unit V : Elements of optimization techniques, single variable function, optimization-direct search, with and without acceleration, method of regular intervals and fibonacci search method, gradient methods.

TEXT BOOK :

1) Digital Computation for Chemical Engineering by Leon Lapidas, McGraw Hill, 1962.

*****

APPENDIX-C

L : Theory Lecture four year B.E. DEGREE COURSE ABBRIVATIONS :-

T : Tutorial SEMESTER PATTERN S - SEMESTER PATTERN

P : Practical SEMESTER : Fifth U - Electronics & Tele.

D : Drawing / Design BRANCH : instrumentation L - Industrial Electronics

I - instrumentation

E - Electrical

Sr. Sub. SUBJECT Teaching Scheme Examination Scheme No. Code L T P/D Theory Practical

No. Total Duration Maximum Total Min. Maximum Total Mininum

Hours/ of Marks Pass Marks Marks Passing

Week Papers Theory College Marks External Internal Marks (Hrs) Papers Assessment

1. 5SI1 Microprocessor and 4 1 2 7 3 80 20 100 40 25 25 50 25

microcontrollers

2. 5SUI2 Power Electronics 4 1 2 7 3 80 20 100 40 25 25 50 25

3. 5SI3 Control System Components 4 1 2 7 3 80 20 100 40 25 25 50 25

4. 5SI4 Material and Process 4 - - 4 3 80 20 100 40 -- -- -- --

5. 5SULI5 Control System Engineering 4 1 - 5 3 80 20 100 40 -- -- -- --

TOTAL 20 4 6 30 500 150

GRAND TOTAL : 650

SEMESTER : SIXTH

BRANCH : instrumentation

Sr. Sub. SUBJECT Teaching Scheme Examination Scheme No. Code L T P/D Theory Practical

No. Total Duration Maximum Total Min. Max. Total Mininum

Hours/ of Marks Pass Marks Marks Passing

Week Papers Theory College Marks External Internal Marks (Hrs) Papers Assessment

1. 6SI1 Analytical Instrumentation 4 1 2 7 3 80 20 100 40 25 25 50 25

2. 6SI2 Basic Industrial Management 4 - - 4 3 80 20 100 40 — — — —

3. 6SI3 Pulse & Digital Circuits 4 1 - 5 3 80 20 100 40 — — — —

4. 6SI4 Electronics Instrumentation 4 1 2 7 3 80 20 100 40 25 25 50 25

5. 6SULI5 Linear Integrated Circuits 4 1 2 7 3 80 20 100 40 25 25 50 25

Engineering

TOTAL 20 4 6 30 500 150

GRAND TOTAL : 650

Note : Industrial visit is compulsory and students are required to submit the report during sixth semester, failing which term will not be granted.